Heroino sintezė iš morfino

[nkd23]

7. Į mišinį (chloroformo tirpalą) dedama aktyvuotos anglies, sugeriančios kietąsias priemaišas, kurios pakartotinai filtruojamos, kol tirpalas tampa skaidrus


ar dirbti su chloroformo dalimi, ar su vandens sluoksniu?

 

[SoldadoDeDrogas]

Depending on the pH - salt will be in the water layer, oil will be with the chloroform. So whatever you originally started with, morphine salt or base, if the pH hasn't changed it should be obvious. I haven't done this but it sounds like it should/will be a salt after addition of the acetate.

 

[Salvador]

G.Patton Big
Ar galite pasakyti tikslų chloroformo kiekį? Ačiū.

 

[G.Patton]

apytiksliai x5 partijos įkrovos gramų

 

[SoldadoDeDrogas]

Yes, you can do small batches at home via the haloform reaction between acetone and sodium hypochlorite:

3 NaOCl + (CH3)2CO → CHCl3 + 2 NaOH + CH3COONa

I believe Uncle Osmo has done this

 

[Chemtrail]

Hey

Swim is trying to understand the science part ... The part were you precipitate the morphine base at ph 8-9 ...

Sooooo the calcium hydroxide (lime) is a strong base (12.4 ph) high pH ; with the opium plant&alkaloids latex water solution mixture ..

Poppy plant material removed via filtration

...

...swim read this quote " Ammonium chloride (NH4Cl) solutions are weakly acidic, typically with a pH between 4.5 and 6.0. "
endquote


... So swim is guessing that adding a water + NH4Cl solution to the strong base (lime) opium mixture will lower the pH


Lower the pH to 8-9
Sit a bit in cool temp and patience to get precipitated morphine base, huh



Wouldn't ammonia gas vapors would emerge from the CaOH and the NH4Cl ??