Leuckart Temp

[Blammo]

I am interested in using the leuckart, with ammonium formate, to form MDA.

What temp should I use? I read about 120 to 130c. Is this correct?

About how long to run the reaction with say 100 grams mdp2p?

 

[Akashic]

much higher or you won’t yield anything. very gradually bring increase temp over few hrs then 6hr@180*c