Question vaihda bentsaldehydi piperonaaliksi Pmk:n luomiseksi.

bitcoinup2020

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Voinko tällä seoksella vaihtaa bentsaldehydin piperonaaliin luodakseni Pmk-glykidaattia?

Reagenssit.

  • Dimetyyliformamidi 900 ml;
  • Bentsaldehydi 300 ml;
  • Etyyli-2-klooripropionaatti 540 g;
  • Bentsyylitrietyyliammoniumkloridi (TEBAC) 32 g;
  • kaliumkarbonaatti 780 g;
  • Natriumhydroksidi (NaOH) 135 g;
  • Tislattu vesi ~1,9 L;
  • Tiivistetty (37 %) vesikloorivetyhappo (HCl) ~250 ml;
Kiitos paljon avusta.
 

HIGGS BOSSON

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rtx1660

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Boss how much piperonal use
Is every step same ?
 

realboss

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Is everything same I mean amount and all steps
 

Newbee

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inst it possible to replace piperonal with something else to create PMK glicydate?
 
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